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Simultaneous Gas-chromatographic Analysis of Heptyl Chloride Heptanesulphonyl Chloride Isomeric Mixtures

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Tazerouti, A. Rahal, S. Soumillion, Jean-Philippe [UCL]

Gas chromatographic analyses of several sulphonyl chlorides were performed without derivatization. Optimized conditions for this analysis were selected and the results controlled by gas chromatography-mass spectrometry. The results obtained were compared with data reported for gas chromatography using derivatization. This method was extended to the simultaneous analysis of isomeric mixtures of n-heptyl chlorides and n-heptanesulphonyl chlorides obtained by the photochemical sulphochlorination of n-heptane.

Document type Article de périodique (Journal article)
Access type Accès restreint
Publication date 1992
Language Anglais
Journal information "Journal of Chromatography A" - Vol. 596, no. 1, p. 132-137 (1992)
Peer reviewed yes
Publisher Elsevier Science Bv (Amsterdam)
issn 0021-9673
e-issn 1873-3778
Publication status Publié
Affiliation UCL
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Bibliographic reference Tazerouti, A. ; Rahal, S. ; Soumillion, Jean-Philippe. Simultaneous Gas-chromatographic Analysis of Heptyl Chloride Heptanesulphonyl Chloride Isomeric Mixtures. In: Journal of Chromatography A, Vol. 596, no. 1, p. 132-137 (1992)
Permanent URL http://hdl.handle.net/2078.1/50470