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Crystal-structure of (2r-asterisk,5r-asterisk)-1-(anilinocarbonyl)-2,5-bis[(1-methoxy-1-methyl)ethyl] Pyrrolidine

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Feneaudupont, J. Declercq, Jean-Paul [UCL] Patiny, L.

C19H30N2O3, M(r) = 334.45, monoclinic, Pc, a = 9.933(2), b = 6.485(2), c = 14.869(2)Angstrom, beta = 99.82(2)degrees, V = 943.8(3)Angstrom(3), Z = 2, D-x = 1.18g.cm(-3), CuK alpha radiation (lambda = 1.54178 Angstrom). The final R indice is 0.042 for 1539 observed reflections.

Document type Article de périodique (Journal article)
Publication date 1995
Language Anglais
Journal information "Societes Chimiques Belges. Bulletin" - Vol. 104, no. 10, p. 625-626 (1995)
Peer reviewed yes
Publisher Soc Chimique Belgique (Brussels)
issn 0037-9646
Publication status Publié
Affiliation UCL
Links
  1. Kawanani, Tetrahedron Lett., 25, 857 (1984)
  2. Ikegami, Tetrahedron, 44, 5333 (1988)
  3. Fuji, Tetrahedron Lett., 31, 3175 (1990)
  4. Gouverneur, Tetrahedron Asymmetry, 1, 363 (1990)
  5. Tetrahedron Letf., 32, 5349 (1991)
  6. Sheldrick, SHELXS86. Program for the Solution of Crystal Structures. (1985)
  7. Sheldrick, SHELXL93. Program for Crystal Structure Refinement. (1993)
  8. Motherwell, PLUTO. Program for plotting molecular and crystal structures (1978)
Bibliographic reference Feneaudupont, J. ; Declercq, Jean-Paul ; Patiny, L.. Crystal-structure of (2r-asterisk,5r-asterisk)-1-(anilinocarbonyl)-2,5-bis[(1-methoxy-1-methyl)ethyl] Pyrrolidine. In: Societes Chimiques Belges. Bulletin, Vol. 104, no. 10, p. 625-626 (1995)
Permanent URL http://hdl.handle.net/2078.1/47704